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61,005 resultsShowing papers similar to Labelling of micro- and nanoplastics for environmental studies: state-of-the-art and future challenges
ClearFrom the synthesis of labeled nanoplastic model materials (isotopic and metallic) to their use in ecotoxicological studies with the detection and quantification analytical methods.
Researchers synthesized isotopically and metallically labeled nanoplastic model materials to enable tracking and quantification of plastic nanoparticles in complex biological and environmental matrices at trace concentrations. The labeled models supported mechanistic studies of nanoplastic fate and exposure by allowing detection at environmentally relevant concentrations not achievable with conventional unlabeled particles.
From the synthesis of labeled nanoplastic model materials (isotopic and metallic) to their use in ecotoxicological studies with the detection and quantification analytical methods.
This study developed labeled nanoplastic model materials using isotopic and metallic tracers to enable tracking and quantification of nanoplastics in complex biological and environmental matrices at environmentally relevant concentrations. Labeled particles allowed localization and measurement of nanoplastics at levels not detectable by conventional methods, advancing mechanistic exposure studies.
Recent Applications in Analytical Techniques of Microplastics
This review surveys analytical methods developed over the past five years for detecting and identifying microplastics, covering fluorescent labeling, spectroscopy, thermal analysis, electrochemistry, mass spectrometry, and chromatography. Researchers found that while each technique has strengths, no single method can fully characterize the diverse types, sizes, and compositions of microplastics found in the environment. The work highlights the need for standardized, comprehensive detection approaches to better monitor and understand microplastic pollution.
Radiolabeling of Micro-/Nanoplastics via In-Diffusion
Researchers developed a radiolabeling method for micro- and nanoplastics by introducing a 64Cu radiotracer into common plastics including polyethylene, polyethylene terephthalate, and others via an in-diffusion technique. The approach provides a sensitive and selective detection strategy for tracking plastic particles in complex ecological media, addressing a key challenge in environmental impact research.
Development and Application of Nanoparticle-Nanopolymer Composite Spheres for the Study of Environmental Processes
This study developed labeled synthetic nanoplastic particles with built-in chemical, isotopic, or fluorescent tracers to allow precise tracking of plastic particle fate and behavior in complex environmental and biological samples. These standardized tracer particles address a key bottleneck in microplastic research by enabling more sensitive and selective detection in real-world matrices.
Fluorescent labelling as a tool for identifying and quantifying nanoplastics
Researchers used fluorescent labeling with four fluorescent molecules to enable detection of nanoplastics from six common polymer types (PP, LDPE, HDPE, PS, PET, PVC) via 3D fluorescence spectral analysis. The method provides a practical approach to identifying and quantifying nanoplastics in samples where conventional spectroscopic methods face sensitivity challenges.
Photoluminescence‐Based Techniques for the Detection of Micro‐ and Nanoplastics
This review examined photoluminescence-based techniques for detecting micro- and nanoplastics, evaluating fluorescent labeling and spectroscopic methods as promising approaches to address the challenge of identifying plastic particles at the smallest scales.
Fabrication and characterization of (fluorescent) model nanoplastics for polymer specific detection
Scientists developed fluorescently labeled model nanoplastics that mimic the properties of real plastic particles, enabling polymer-specific identification at very small scales. These standardized reference particles are a key research tool because nanoplastics are otherwise extremely difficult to detect and characterize in environmental samples.
A review on analytical performance of micro- and nanoplastics analysis methods
This review evaluated the analytical methods currently available for detecting and measuring micro- and nanoplastics in various environments. Researchers compared techniques based on their accuracy, sensitivity, and practical limitations, noting that particle size and the complexity of the surrounding material significantly affect method performance. The study identifies key challenges and provides guidance on selecting appropriate analytical approaches for different types of plastic pollution research.
Fluorescent plastic nanoparticles to track their interaction and fate in physiological environments
This study developed fluorescently labeled plastic nanoparticles made from PET, polypropylene, and polystyrene that can be tracked in biological environments to study how nanoplastics are taken up and processed by living organisms. Having trackable model nanoplastics is an important tool for understanding how these particles move through tissues and food chains.
Methods and challenges in the detection of microplastics and nanoplastics: a mini‐review
This review evaluated the strengths and weaknesses of analytical methods used to detect and identify microplastics and nanoplastics, including microscopy, spectroscopy, and mass spectrometry techniques. Researchers identified key challenges such as distinguishing genuine environmental microplastics from contamination introduced during sample collection and processing. The study provides recommendations for improving data quality and reliability in microplastic research.
Labeling Microplastics with Fluorescent Dyes for Detection, Recovery, and Degradation Experiments
Researchers optimized fluorescent dye staining protocols for labeling 17 different plastic polymer types using four textile dyes and Nile red for detection, recovery, and degradation experiments. Dye performance varied significantly by polymer type and staining conditions, and standardized protocols were recommended to improve comparability across microplastic studies.
Fluorescent Tagging of Polymer Particles with PBN for the Detection of Microplastics in Personal Care Goods
Researchers used fluorescent labeling to detect microplastic particles in personal care products, a common but undermonitored source of plastic pollution. The method proved effective for identifying small polymer particles in consumer goods.
Nanoplastic Labelling with Metal Probes: Analytical Strategies for Their Sensitive Detection and Quantification by ICP Mass Spectrometry
Researchers developed metal probe labelling strategies to enable sensitive detection and quantification of nanoplastics by ICP mass spectrometry, overcoming the challenge that nanoplastics are too small and carbon-rich for conventional analytical techniques to distinguish.
Challenges and Advances in Analytical Techniques to Detect Micro- and Nanoplastics
This research review summarizes the current methods scientists use to detect and study microplastics and nanoplastics - tiny plastic particles that can get into our environment, food, and bodies. The authors explain that identifying these extremely small plastic pieces is very challenging and requires advanced laboratory techniques to understand what types of plastics they are and how much is present. Better detection methods are important because we need to understand how much plastic pollution we're exposed to and its potential effects on human health.
Illuminating the Invisible: Fluorescent Probes as Emerging Tools for Micro/Nanoplastic Identification
This review traces the development of fluorescent probes for detecting micro- and nanoplastics in environmental samples, from early hydrophobic stains to advanced molecular designs with improved selectivity. Researchers found that newer probe technologies offer significant advantages in sensitivity and throughput compared to conventional detection methods like FTIR and Raman spectroscopy. The study highlights remaining challenges including standardizing protocols across different environmental matrices and improving detection of the smallest nanoplastic particles.
Chemical Analysis of Microplastics and Nanoplastics: Challenges, Advanced Methods, and Perspectives
This review covers the latest laboratory methods for detecting and measuring microplastics and nanoplastics in environmental samples like water, food, and air. Identifying these tiny particles is extremely challenging because they vary enormously in size, shape, and plastic type, and concentrations can differ by billions of times between samples. Better standardized detection methods are essential for accurately understanding how much microplastic humans are actually exposed to.
New Analytical Approaches for Effective Quantification and Identification of Nanoplastics in Environmental Samples
This review assessed new analytical approaches for quantifying and identifying nanoplastics in environmental samples, highlighting fundamental challenges in detection due to their small size and the need for improved methods to understand nanoplastic contamination levels.
The micro-, submicron-, and nanoplastic hunt: A review of detection methods for plastic particles
This review systematically summarizes detection and characterization methods for micro-, submicron-, and nanoplastics, providing recommendations for method validation, standardization, and analytical pathways suited to different sample types and research goals.
A critical comparison of the main characterization techniques for microplastics identification in an accelerated aging laboratory experiment
This paper critically compared the main spectroscopic and microscopic characterization techniques used to identify microplastics in environmental samples, evaluating their strengths, limitations, and suitability for different matrices. The review highlighted the need for standardized methods to improve comparability across microplastic studies.
Spectro‐Microscopic Techniques for Studying Nanoplastics in the Environment and in Organisms
This review examined spectro-microscopic techniques available for detecting and studying nanoplastics in environmental and biological samples. The study highlights that detecting nanoplastics remains challenging because their small size falls below the detection limits of common analytical tools, and their chemical composition is similar to organic matrices, making identification difficult.
New fluorescence labeling isotactic polypropylenes as a tracer: a proof of concept
Researchers developed fluorescence-labeled isotactic polypropylene tracer materials as a proof of concept for detecting polypropylene-derived microplastic pollutants in organic tissues, enabling tracking of PP-sourced particles in biological samples.
Tracking of realistic nanoplastics in complicated matrices by iridium element labeling and inductively coupled plasma mass spectroscopy
Researchers developed a protocol to track realistic nanoplastics in environmental and biological samples by labeling them with an iridium-containing agent and detecting them via inductively coupled plasma mass spectroscopy, demonstrating stable tracking across complex matrices.
Fluorescent Dyes for Visualizing Microplastic Particles and Fibers in Laboratory-Based Studies
Researchers developed a heat-mediated dyeing protocol that allows fluorescent dyes to be stably incorporated into a variety of microplastic types and shapes for use in laboratory tracking experiments. The method works across multiple common polymer types and particle morphologies, extending the tool beyond the polystyrene spheres that have dominated previous studies. The protocol enables researchers to better study the environmental fate and biological uptake of realistically shaped microplastics.