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61,005 resultsShowing papers similar to Refined Analysis of Microplastics: Integrating Infrared and Raman Spectroscopy
ClearOptimizing microplastic analysis through comparative FTIR and raman spectroscopy: Addressing challenges in environmental degradation studies
This study optimized microplastic analysis by comparing FTIR and Raman spectroscopy approaches for identifying degraded polymer particles in environmental samples where photooxidation and mechanical fragmentation have altered spectral signatures. A combined spectroscopy approach outperformed either technique alone for accurately identifying degraded microplastics in complex environmental matrices.
Optimizing microplastic analysis through comparative FTIR and raman spectroscopy: Addressing challenges in environmental degradation studies
Researchers compared FTIR and Raman spectroscopy for analyzing degraded microplastic polymers in environmental samples, evaluating how polymer aging affects identification accuracy. The study found that spectral databases based on pristine polymers can misidentify weathered microplastics, calling for updated reference libraries.
Analytical tools in advancing microplastics research for identification and quantification across environmental media: from sample to insight
Researchers reviewed the analytical tools most commonly used for identifying and quantifying microplastics, focusing on FTIR and Raman spectroscopy as the two primary methods. The review compared their strengths and limitations and provided guidance for choosing between them based on particle size, sample matrix, and research objectives.
Characterization of microplastics in environment by thermal gravimetric analysis coupled with Fourier transform infrared spectroscopy
Researchers developed a method combining thermogravimetric analysis (TGA) with Fourier transform infrared spectroscopy (FTIR) to identify and quantify microplastics in environmental samples, demonstrating that the combined temperature profiles and absorption spectra provide greater discriminatory power than either technique alone.
Insights Into Microplastics Pollution in Aquatic Ecosystem: a Short Review of Sampling and Analysis Methods
This review summarizes current methods for sampling and analyzing microplastics in rivers and estuaries, including techniques like FTIR and Raman spectroscopy for polymer identification. The authors highlight the need for standardized sampling and analysis methods to ensure that microplastic data across different studies are reliable and comparable.
Application of fluorescent microscopy and Fourier-transform infrared spectroscopy for analysis of microplastics in Can Gio seawater
Researchers validated the combined use of fluorescent microscopy and Fourier-transform infrared spectroscopy for detecting and identifying microplastics in marine environmental samples. The dual-technique approach improved detection sensitivity and chemical identification accuracy compared to either method used alone.
Comparison of Raman and Fourier Transform Infrared Spectroscopy for the Quantification of Microplastics in the Aquatic Environment
Microplastics from North Sea surface waters were analyzed by both Raman and FTIR spectroscopy across two size fractions, with automated Raman quantifying approximately twice as many particles ≤500 μm as FTIR imaging, but similar results for larger particles. The comparison study identifies key trade-offs between the two techniques and demonstrates that method choice significantly affects microplastic abundance estimates.
Contributions of Fourier transform infrared spectroscopy in microplastic pollution research: A review
This review covers advances in Fourier transform infrared (FTIR) spectroscopy techniques — including chemical imaging — for identifying polymer types in microplastic samples and tracing their fate in different environmental matrices.
Analysis of environmental microplastics by vibrational microspectroscopy: FTIR, Raman or both?
This study reviewed analytical methods for environmental microplastic analysis using vibrational microspectroscopy — comparing FTIR, Raman, and related techniques — and provided guidance on method selection for different sample types and research questions.
Combination of Micro‐Raman and Infrared Spectroscopy to Identify Intriguing Case of Aged Microplastics of Estuarine Sediments
Researchers used a combination of Raman and infrared spectroscopy to identify aged microplastics in mangrove sediments near Santos, Brazil, one of the most biodiverse regions in the world. The dual-technique approach was able to identify not only the plastic polymers but also chemical additives like blue ink and green dye embedded in the particles. The study demonstrates how combining analytical methods improves the accuracy of microplastic identification in complex environmental samples.
Analysis of microplastics of a broad size range in commercially important mussels by combining FTIR and Raman spectroscopy approaches
Researchers developed an approach combining FTIR and Raman spectroscopy to analyze microplastics across a broad size range in commercially important mussels. They found that using both techniques together captured a wider spectrum of particle sizes and polymer types than either method alone. The study provides a more complete picture of microplastic contamination in seafood and highlights the importance of using complementary analytical methods for accurate assessment.
The development of an analytical procedure for the determination of microplastics in freshwater ecosystems
Researchers developed an improved analytical procedure for detecting and identifying microplastics in freshwater environments. The method combines careful sample preparation with advanced instrumental techniques like infrared and Raman spectroscopy. The study highlights the importance of standardized methods to ensure that microplastic measurements across different studies are reliable and comparable.
Promising techniques and open challenges for microplastic identification and quantification in environmental matrices
This review assessed current and emerging techniques for microplastic identification and quantification in environmental matrices, highlighting advantages and limitations of methods including FTIR, Raman spectroscopy, and pyrolysis-GC/MS.
Advanced analytical techniques for microplastics in the environment: a review
Researchers reviewed the most advanced laboratory tools for detecting and identifying microplastics in environmental samples — including infrared spectroscopy, Raman spectroscopy, and pyrolysis gas chromatography — summarizing the strengths and weaknesses of each technique to help researchers choose the right method for accurate microplastic analysis.
Raman Spectroscopy and Machine Learning for Microplastics Identification and Classification in Water Environments
Researchers combined Raman spectroscopy with machine learning algorithms for automated identification and classification of microplastics in water environments, achieving high accuracy in distinguishing different polymer types based on spectral fingerprints.
Comparison of μ-ATR-FTIR spectroscopy and py-GCMS as identification tools for microplastic particles and fibers isolated from river sediments
Researchers compared two identification methods — micro-ATR-FTIR spectroscopy and pyrolysis-GC-MS — for characterizing microplastics extracted from river sediments, finding that the methods generally agreed on dominant polymers but differed in sensitivity to certain types. The comparison provides practical guidance for choosing analytical methods in freshwater microplastic monitoring programs.
Harmonizing infrared spectroscopic techniques for microplastic identification: a comparative evaluation of ATR and µFTIR transmission and reflection modes
Researchers systematically compared the performance of Attenuated Total Reflectance (ATR) and micro-Fourier Transform Infrared Spectroscopy (muFTIR) in both transmission and reflection modes for identifying microplastics from twelve common real-world plastic products, providing guidance on optimizing spectroscopic technique selection.
Optical photothermal infrared spectroscopy with simultaneously acquired Raman spectroscopy for two-dimensional microplastic identification
Researchers demonstrated that optical photothermal infrared spectroscopy combined with simultaneous Raman acquisition enables more reliable two-dimensional microplastic identification, overcoming limitations of individual FTIR or Raman techniques alone.
An investigation on the applications of advanced Infrared Spectroscopy, Spectral Imaging and Machine Learning for Polymer Characterization, including microplastics
This study integrated advanced infrared spectroscopy, spectral imaging, chemometrics, and machine learning to identify and characterize microplastics and polymer degradation products. The combination of techniques improved both the accuracy and throughput of MP analysis compared to conventional methods.
Sequential quantification of number and mass of microplastics in municipal wastewater using Fourier-transform infrared spectroscopy and pyrolysis gas chromatography-mass spectrometry
Researchers developed a sequential analytical method combining FTIR microscopy and pyrolysis-GC/MS to identify and quantify microplastics in municipal wastewater samples, with FTIR providing polymer type and physical dimensions and Pyr-GC/MS providing chemical composition. The combined approach improves accuracy compared to using either method alone.
The effect of weathering environments on microplastic chemical identification with Raman and IR spectroscopy: Part I. polyethylene and polypropylene
Researchers compared Raman and IR spectroscopy for identifying weathered polyethylene and polypropylene microplastics, finding that weathering significantly alters surface chemistry and that Raman spectroscopy is more robust for identifying heavily weathered samples than IR spectroscopy.
A novel method for purification, quantitative analysis and characterization of microplastic fibers using Micro-FTIR
Researchers developed an improved method for purifying, quantifying, and characterizing microplastic fibers using micro-FTIR spectroscopy, addressing the challenge that fibers are harder to process and identify than other microplastic shapes. The method improvements enable more accurate characterization of this common but technically challenging category of environmental microplastics.
Investigation of new analysis methods for simultaneous and rapid identification of five different microplastics using ATR-FTIR spectroscopy and chemometrics
Researchers developed and evaluated ATR-FTIR spectroscopy combined with chemometric analysis for simultaneous rapid identification of five common microplastic polymer types in water samples. The method achieved high classification accuracy across polymer types, offering a faster and more automated alternative to conventional single-polymer identification approaches.
Analytical and Detection Techniques for Microplastics
This chapter reviewed analytical and detection techniques for microplastics across environmental matrices, covering sampling strategies, separation methods, and identification tools including FTIR and Raman spectroscopy, with discussion of their sensitivity, cost, and suitability for different environmental monitoring applications.