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20 resultsShowing papers similar to From qualitative to quantitative measurement of small microplastics using multi-detector field flow fractionation coupled offline to microscopy and raman spectroscopy
ClearFrom qualitative to quantitative measurement of small microplastics using multi-detector field flow fractionation coupled offline to microscopy and raman spectroscopy
This study developed an analytical method combining multi-detector field flow fractionation with offline microscopy and Raman spectroscopy to move from simply identifying microplastics to accurately measuring their quantity in small size ranges. Improved quantification methods are critical because current inconsistencies in measurement approaches make it difficult to set health-based exposure limits or compare contamination levels across studies.
Systematic quantitation for microplastics and nanoplastics based on size-fractionated filtration hyphenated to Raman/SERS and slope-matching strategy
Researchers developed a systematic method for accurately measuring micro- and nanoplastics using size-fractionated filtration combined with Raman and surface-enhanced Raman spectroscopy. The approach addresses the challenge of quantifying plastic particles with heterogeneous size distributions, offering a more reliable strategy for environmental monitoring.
Flow Raman Spectroscopy for the Detection and Identification of Small Microplastics
Researchers developed a new method using flow Raman spectroscopy to detect and identify individual microplastic particles as small as 4 micrometers while they move through water. Unlike current methods that require complex sample preparation, this technique could work in real time for monitoring food and drinking water quality. The method can distinguish between different plastic types even after they have been weathered by the environment.
Analytical tools in advancing microplastics research for identification and quantification across environmental media: from sample to insight
Researchers reviewed the analytical tools most commonly used for identifying and quantifying microplastics, focusing on FTIR and Raman spectroscopy as the two primary methods. The review compared their strengths and limitations and provided guidance for choosing between them based on particle size, sample matrix, and research objectives.
An effective solution to simultaneously analyze size, mass and number concentration of polydisperse nanoplastics in a biological matrix: asymmetrical flow field fractionation coupled with a diode array detector and multiangle light scattering
Researchers developed an asymmetrical flow field-flow fractionation method coupled with a diode array detector and multiangle light scattering to simultaneously measure the size, mass, and number concentration of polydisperse nanoplastics in biological matrices, providing a more accurate tool for assessing nanoplastic pollution levels.
Improved Reliability of Raman Spectroscopic Imaging of Low-Micrometer Microplastic Mixtures in Lake Water by Fractionated Membrane Filtration
Researchers developed an analytical method coupling fractionated membrane filtration with Raman microspectroscopy to reliably quantify low-micrometer microplastics (1-10 micrometers) in lake water, achieving over 90% recovery of polystyrene and PMMA particles and improving image quality by separating particles into distinct size fractions.
Analytical tools in advancing microplastics research for identification and quantification across environmental media: from sample to insight
This review surveys analytical techniques used in microplastic research, covering sampling, extraction, and identification methods including FTIR, Raman spectroscopy, and pyrolysis-GC/MS, highlighting trade-offs between throughput, sensitivity, and particle size detection limits.
Assessing diversity, abundance, and mass of microplastics (~ 1–300 μm) in aquatic systems
Researchers developed improved methods for quantifying very small microplastic particles (roughly 1 to 300 micrometers) in freshwater systems, showing that conventional sampling dramatically underestimates plastic particle counts. Accurately measuring this smaller size fraction is critical for understanding real-world microplastic concentrations and their biological impacts.
Online Coupling of Field-Flow Fractionation with Raman Microspectroscopy Enables the Advanced Study of Nanoplastics Directly in Food
Researchers developed an online coupling of field-flow fractionation with Raman microspectroscopy to enable direct detection and characterisation of nanoplastics in complex food matrices, overcoming limitations of existing methods that require laborious sample preparation.
Application of raman micro-spectroscopy for quantitative microplastics analysis
This review examines the application of Raman microspectroscopy for quantitative microplastic analysis, emphasizing the technique's ability to detect particles down to 1 micron - the smallest size range posing the highest environmental and health risk. The authors highlight Raman microspectroscopy's advantages over other methods for measuring microplastic concentrations across diverse environmental matrices.
Development of automated microplastic identification workflow for Raman micro-imaging and evaluation of the uncertainties during micro-imaging
Researchers developed an automated identification workflow for Raman micro-imaging of microplastics, validating it with artificial samples of known polymer microspheres and showing that the workflow reliably identifies plastic type and estimates particle size across a range of sizes.
Nanoplastic Analysis by Online Coupling of Raman Microscopy and Field-Flow Fractionation Enabled by Optical Tweezers
Researchers developed a new analytical technique for detecting nanoplastics by combining field-flow fractionation with online Raman microspectroscopy, using optical tweezers to trap particles and overcome weak scattering signals. The method successfully identified polymer and inorganic particles ranging from 200 nm to 5 micrometers at concentrations around 1 mg/L.
The power of a multi-technique approach for the reliable quantification of microplastics in water
Researchers applied a multi-technique analytical approach combining several spectroscopic and microscopic methods to improve the reliability of microplastic quantification in environmental samples. The combined approach reduced false positives and improved polymer identification accuracy compared to any single method used alone.
Particle size-dependent quantitative and qualitative differences of common microplastic detection procedures: Nile Red-assisted fluorescence microscopy and confocal micro-Raman spectroscopy
Researchers compared confocal micro-Raman spectroscopy and Nile Red-assisted fluorescence microscopy for detecting microplastics across different size classes. Both methods delivered better agreement for larger particles (>100 µm), with particle size significantly influencing the percentage differences between methods, underscoring the need for size-specific method validation.
Towards a quantitative approach for the accurate analysis of blended microplastics based on 3-D micro-Raman spectroscopy
Researchers developed a quantitative 3D micro-Raman spectroscopy approach for accurately analyzing blended microplastic particles composed of multiple polymer types, addressing the challenge that environmentally released microplastics often originate from complex multi-polymer blended materials.
Matrix OverloadingEffects on Size-Resolved Quantificationof Low-Concentration Nanoplastics in Complex Environmental MatricesUsing Asymmetric Flow Field-Flow Fractionation
Researchers developed a size-resolved nanoplastic quantification method using asymmetric flow field-flow fractionation with on-channel preconcentration, identifying and characterizing matrix overloading effects that cause analytical artifacts when measuring nanoplastics in complex environmental water samples.
Matrix Overloading Effects on Size-Resolved Quantification of Low-Concentration Nanoplastics in Complex Environmental Matrices Using Asymmetric Flow Field-Flow Fractionation
Researchers developed a size-resolved method for quantifying nanoplastics in the 20-200 nm range in environmental water samples using asymmetric flow field-flow fractionation. The study identified important analytical artifacts from matrix overloading effects that can occur when measuring low-concentration nanoplastics in complex environmental samples, providing guidance for more accurate quantification methods.
How to Identify and Quantify Microplastics and Nanoplastics Using Raman Imaging?
This paper reviews advances in Raman imaging as a method for identifying and quantifying microplastics and nanoplastics in environmental samples, discussing current protocols, analytical challenges, and the need for standardization.
Promising techniques and open challenges for microplastic identification and quantification in environmental matrices
This review assessed current and emerging techniques for microplastic identification and quantification in environmental matrices, highlighting advantages and limitations of methods including FTIR, Raman spectroscopy, and pyrolysis-GC/MS.
Analytical methods for microplastics in the environment: a review
Researchers reviewed classical and advanced analytical methods for detecting microplastics in the environment. The methods covered include visual analysis, electron microscopy, infrared and Raman spectroscopy, thermal analysis, mass spectrometry, and flow cytometry, providing a comprehensive overview of available tools for microplastic identification and quantification.