0
Article ? AI-assigned paper type based on the abstract. Classification may not be perfect — flag errors using the feedback button. Tier 2 ? Original research — experimental, observational, or case-control study. Direct primary evidence. Sign in to save

Instrumental analysis of microplastics—benefits and challenges

Analytical and Bioanalytical Chemistry 2018 238 citations ? Citation count from OpenAlex, updated daily. May differ slightly from the publisher's own count. Score: 45 ? 0–100 AI score estimating relevance to the microplastics field. Papers below 30 are filtered from public browse.
Sven Huppertsberg, Thomas P. Knepper

Summary

This review evaluates the benefits and challenges of instrumental analytical methods for microplastic analysis, including spectroscopic techniques (FTIR, Raman) and thermal methods (Py-GC-MS, TED-GC-MS), discussing their applicability to different sample types and size ranges. The paper serves as a comprehensive guide for researchers selecting methods to characterize microplastics in environmental samples.

There is a high demand for easy, cheap, comparable, and robust methods for microplastic (MP) analysis, due to the ever-increasing public and scientific interest in (micro-) plastic pollution in the environment. Today, a multitude of methodologies for sampling, sample preparation, and analysis of MPs are in use. This feature article deals with the most prominent detection methods as well as with sampling strategies and sample preparation techniques. Special emphasis is on their benefits and challenges. Thus, spectroscopic methods, coupled with microscopy, require time-consuming sample preparation and extended measurement times, whereas thermo-analytical methods are faster but lack the ability to determine the size distribution in samples. To that effect, most of the described methods are applicable depending on the defined analytical question. Graphical abstract ᅟ.

Sign in to start a discussion.

More Papers Like This

Article Tier 2

The Advancements and Detection Methodologies for Microplastic Detection in Environmental Samples

This review chapter examines destructive and non-destructive analytical methods for detecting and identifying microplastics in environmental samples, covering thermal analysis, GC-MS, FTIR spectroscopy, and Raman spectroscopy. The authors evaluate each technique's sensitivity, applicability across sample matrices, and limitations, aiming to guide method selection for environmental monitoring and research.

Article Tier 2

Analytical tools in advancing microplastics research for identification and quantification across environmental media: from sample to insight

This review surveys analytical techniques used in microplastic research, covering sampling, extraction, and identification methods including FTIR, Raman spectroscopy, and pyrolysis-GC/MS, highlighting trade-offs between throughput, sensitivity, and particle size detection limits.

Article Tier 2

Analytical tools in advancing microplastics research for identification and quantification across environmental media: from sample to insight

Researchers reviewed the analytical tools most commonly used for identifying and quantifying microplastics, focusing on FTIR and Raman spectroscopy as the two primary methods. The review compared their strengths and limitations and provided guidance for choosing between them based on particle size, sample matrix, and research objectives.

Article Tier 2

Promising techniques and open challenges for microplastic identification and quantification in environmental matrices

This review assessed current and emerging techniques for microplastic identification and quantification in environmental matrices, highlighting advantages and limitations of methods including FTIR, Raman spectroscopy, and pyrolysis-GC/MS.

Article Tier 2

Analysis of environmental microplastics by vibrational microspectroscopy: FTIR, Raman or both?

This study reviewed analytical methods for environmental microplastic analysis using vibrational microspectroscopy — comparing FTIR, Raman, and related techniques — and provided guidance on method selection for different sample types and research questions.

Share this paper