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Mesoscopic Strain Fields Measurement During the Allotropic α − γ Transformation in High Purity Iron

Experimental Mechanics 2019 5 citations ? Citation count from OpenAlex, updated daily. May differ slightly from the publisher's own count. Score: 20 ? 0–100 AI score estimating relevance to the microplastics field. Papers below 30 are filtered from public browse.
Nicolas Bruzy, Michel Coret, Michel Coret, Bertrand Huneau, Guillaume Kermouche, Marilyne Mondon, Marilyne Mondon, Emmanuel Bertrand, Laurent Stainier

Summary

In situ synchrotron X-ray diffraction was used to measure mesoscopic strain fields during the alpha-to-gamma allotropic phase transformation in iron, capturing how the volume change between ferrite and austenite creates microplastic accommodation strains at the grain scale. The measurements provide direct experimental evidence for transformation-induced microstructural stresses in iron.

The allotropic phase change from ferrite to austenite represents a moment of massive interplay between the microstructural and mechanical states of iron. The difference of compacity between the two phases induces a microplastic accommodation in the material at grain scale. However, mechanical heterogeneities resulting from the transformation process remain challenging to characterise due to the high temperature conditions it is associated with. We developed experimental equipment for in situ observation of α − γ and γ − α transformations. Images of the surface of an iron sample taken by an optical camera were used as input for a Digital Image Correlation (DIC) routine. Special care was taken to maximize image resolution to capture sub-grain phenomena. Observations show that, at the mesoscopic scale, shear strain fields exhibit strong localisations that are evidence of transformations that are occurring.

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