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Hydrophobicity–water/air–based enrichment cell for microplastics analysis within environmental samples: A proof of concept

MethodsX 2019 24 citations ? Citation count from OpenAlex, updated daily. May differ slightly from the publisher's own count.
Gerrit Renner, Alexander Nellessen, Alexander Schwiers, Mike Wenzel, Mike Wenzel, Torsten C. Schmidt, Jürgen Schram

Summary

Researchers developed a new microplastic separation device that uses the hydrophobic properties of plastic particles combined with fine air bubbles to quickly and effectively extract microplastics from sediment and soil samples. The new method avoids harsh solvents that can degrade microplastic particles and offers a faster alternative to existing separation techniques.

Study Type Environmental

The analysis of microplastics in sediments, soils or beach samples is commonly paired with a separation step to enrich microplastics or to remove non-plastics, respectively. Those steps are often very time consuming and are performed in presence of high concentrated solvents. The latter are also suspected to corrode or decompose the analyte particles, which hamper further identification processes. This paper describes a new fast and effective microplastics separation apparatus for analytical issues that was based on hydrophobic adhesion of microplastics and fine air bubbles. The presented prototype could successfully enrich over 90 % of 30ppm microplastics in 200 g sand in 20 min. Additionally, it could be demonstrated that the new separation technique was very suitable for further microplastics identification by FTIR microscopy. In this context, a sample with different polymers and matrix components was analyzed and the results were presented within this article. •.•.• 20 min .

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