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Aqueous degradability of water-soluble, thioester-containing polyacrylamides with UCST-type behaviour in salt solutions obtained by rROP

Chemical Communications 2024 3 citations ? Citation count from OpenAlex, updated daily. May differ slightly from the publisher's own count. Score: 40 ? 0–100 AI score estimating relevance to the microplastics field. Papers below 30 are filtered from public browse.
Thomas J. Neal, Julien Nicolas

Summary

Researchers synthesized water-soluble polyacrylamide copolymers containing thioester bonds designed to degrade rapidly in water when exposed to common household chemicals like bleach, caustic soda, or amino acids, reducing molecular weight by up to 90%. Designing degradability directly into water-soluble polymers — which are widely used in industry and agriculture and can contribute to microplastic-like pollution — is a promising strategy for preventing their persistence in aquatic environments.

We report the successful synthesis of hydrophilic thioester-containing polyacrylamide copolymers by the RAFT and free-radical copolymerisation of dibenzo[c,e]oxepane-5-thione with either acrylamide or N-isopropylacrylamide. These copolymers efficiently degrade in aqueous solutions of sodium hydroxide, isopropylamine, L-cysteine, and household bleach, reducing the weight-average molecular weight by up to ∼90%.

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