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High throughput application of ASTM D8332: Detailed prototype design and operating conditions for microplastic sampling of riverine systems

MethodsX 2024 3 citations ? Citation count from OpenAlex, updated daily. May differ slightly from the publisher's own count.
Jeremiah Bryksa, Patric McGlashan, Nadia Stelck, Jon Wong, Andrew Anderson-Serson, Matthew B. Hart, Trace Malcom, Bob Battle, Paolo Mussone

Summary

Researchers designed and tested a high-throughput pumping system based on the ASTM D8332 standard as an alternative to net-based sampling for collecting microplastics from turbulent, sediment-heavy freshwater rivers and stormwater systems. Improving sampling methodology is critical for generating reliable data on microplastic concentrations in river systems, which are a major pathway for plastic pollution reaching the ocean.

Study Type Environmental

Microplastic sampling strategies for aquatic systems commonly employ small mesh nets to collect suspended microparticles. These methods work well for marine sampling campaigns; however, complex water systems such as freshwater rivers, effluent discharges, and stormwater ponds characterized by high total suspended solids and fast-moving water can cause the nets to clog, rip, or tear. Published in 2020, ASTM D8332 is an alternative approach to sampling complex water systems for microplastics involving pumping large volumes of water across a cascading stack of sieves to collect suspended particles. Here we show that ASTM D8332 can be applied to sample freshwater rivers for microplastic collection. A high throughput sampling prototype developed in this work is capable of pumping 1500 L of river water in 45 min to collect particles as small as 45 µm. The system is lightweight, modular, and easily transportable. It has a discrete power supply, allowing for the collection of microplastics anywhere along the river, including municipal discharges. The design minimizes the amount of plastic in the flow path and provides a practical way to measure field contamination. Finally, we outline lessons learned through extensive field trials and testing using this system sampling the North Saskatchewan River in Edmonton, Alberta. •Existing small mesh nets face limitations in freshwater rivers, encountering clogging and tearing issues from high suspended solids and fast moving water.•Using a standardized method, ASTM D8332 - a pumping-based approach is efficient for microplastic collection in freshwater rivers.•Lightweight, modular, plastic free prototype system pumps 1500 L of river water in 45 min, collecting particles as small as 45 µm. Successfully tested in the North Saskatchewan River.

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